Data Validation

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11 Revision 0 Validated Sample Result Forms: Analysis Method 350.1 Sample Name CC06092120151300 Lab Sample Name: 680-117013-1 Analyte Ammonia Total/Dissolved T CAS No CC06092120151300 Lab Sample Name: 680-117013-1 Nitrogen, Kjeldahl Total/Dissolved T CAS No MDL 1.6 0.71 Result Units mg/Kg Lab Qualifier U Validation Validation Qualifier Notes U Matrix Type: Solid Result Value 140 Reporting Limit MDL 230 140 Result Units mg/Kg Lab Qualifier U Validation Validation Qualifier Notes U 6010C Sample Name CC06092120151300 Lab Sample Name: 680-117013-1 Analyte 0.71 Reporting Limit Sample Date: 9/21/2015 1:00:00 PM STL00296 Analysis Method Result Value 351.2 Sample Name Analyte Matrix Type: Solid Sample Date: 9/21/2015 1:00:00 PM 7664-41-7 Analysis Method 680-117013-1 Total/Dissolved Matrix Type: Solid Sample Date: 9/21/2015 1:00:00 PM CAS No Result Value Reporting Limit MDL Result Units Lab Qualifier Aluminum T 7429-90-5 3600 1000 160 mg/Kg Antimony T 7440-36-0 42 100 42 mg/Kg U Arsenic T 7440-38-2 340 100 41 mg/Kg F2 Validation Validation Qualifier Notes U Barium T 7440-39-3 8.2 51 8.2 mg/Kg U F1 U Beryllium T 7440-41-7 0.19 2.1 0.051 mg/Kg J J Cadmium T 7440-43-9 5.1 26 5.1 mg/Kg U F1 U Calcium T 7440-70-2 270 2600 270 mg/Kg U U Chromium T 7440-47-3 16 51 11 mg/Kg J J Cobalt T 7440-48-4 5.1 51 5.1 mg/Kg U U Copper T 7440-50-8 1800 130 8.7 mg/Kg F2 J Iron T 7439-89-6 530000 1000 270 mg/Kg Lead T 7439-92-1 80 51 17 mg/Kg Magnesium T 7439-95-4 100 260 46 mg/Kg J J Manganese T 7439-96-5 210 51 5.1 mg/Kg Nickel T 7440-02-0 20 210 20 mg/Kg U U Potassium T 7440-09-7 13 510 13 mg/Kg U U Selenium T 7782-49-2 50 130 50 mg/Kg U F1 U Silver T 7440-22-4 3.1 51 3.1 mg/Kg U U Sodium T 7440-23-5 2500 10000 2500 mg/Kg U F1 U Thallium T 7440-28-0 31 130 31 mg/Kg U U Vanadium T 7440-62-2 71 5.1 0.51 mg/Kg Friday, September 25, 2015 J E E Page 1 of 6 Analysis Method Zinc 6010C T 7440-66-6 Analysis Method CC06092120151300 Lab Sample Name: 680-117013-1 Mercury Total/Dissolved T CAS N

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