Method Validation
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Fortification level (mg/kg) Aclonifen Acrinathrin Benalaxyl Bifenthrin Bitertanol Bromophos-ethyl Bromopropylate Carbofenthion Carbofuran Chlorfenvinphos 0.011 0.022 0.217 LOD RSDr, 15 8 3 0.007 RSDR, Recovery, 32 74 14 82 8 98 RSDr, 5 14 5 RSDR, Recovery, 26 95 23 93 9 84 RSDr, 12 4 5 RSDR, Recovery, 20 153 9 131 7 99 RSDr, 46 12 1 RSDR, Recovery, 33 125 17 108 11 94 RSDr, 14 24 7 RSDR, Recovery, 22 90 18 95 10 102 RSDr, 10 9 4 RSDR, Recovery, 40 94 20 92 11 93 RSDr, 12 4 6 RSDR, Recovery, 26 111 19 104 11 94 RSDr, 16 15 5 RSDR, Recovery, 21 122 29 102 12 103 RSDr, 17 3 RSDR, Recovery, 17 114 5 109 9 5 2 27 118 13 113 7 105 RSDr, RSDR, Recovery, 0.008 0.046 0.012 0.006 0.011 0.009 0.008 0.013 0.009 National Food Institute, The Danish Technical University 9 Fortification level (mg/kg) Chlorobenzilate RSDr, RSDR, Recovery, Chloropropylate RSDr, RSDR, Recovery, Chlorpyriphos Chlorpyriphos-methyl Chlorthal-dimethyl Cyprodinil Dialifos Diclofenthion Diethofencarb Dioxathion 0.022 0.217 LOD 6 3 2 0.005 16 104 14 104 6 99 9 3 2 18 102 14 104 6 99 RSDr, 5 RSDR, Recovery, 19 92 RSDr, 7 6 5 RSDR, Recovery, 31 142 17 117 6 101 RSDr, 14 16 2 RSDR, Recovery, 27 89 24 89 31 89 RSDr, 9 6 2 RSDR, Recovery, 9 93 9 96 7 97 RSDr, 9 9 9 20 110 8 111 10 104 RSDr, 14 5 RSDR, Recovery, 18 130 7 101 RSDR, Recovery, Diazinon 0.011 RSDr, 11 12 6 RSDR, Recovery, 11 95 12 92 6 96 RSDr, 7 6 23 RSDR, Recovery, 8 103 8 102 34 92 RSDr, 27 7 3 RSDR, Recovery, 29 85 20 103 9 100 0.006 0.11 0.012 0.007 0.003 0.007 0.042 0.003 0.003 0.013 National Food Institute, The Danish Technical University 10 Fortification level (mg/kg) Ethion Etrimfos Fenarimol Fenchlorphos 0.011 0.022 0.217 LOD RSDr, 14 9 5 0.004 RSDR, Recovery, 13 94 10 100 6 102 RSDr, 8 12 5 RSDR, Recovery, 29 192 23 143 12 102 RSDr, 27 11 8 RSDR, Recovery, 29 128 16 113 9 100 7 7 3 38 141 19 116 5 98 6 5 5 RSDR, Recovery, 17 142 9 118 6 104 RSDr, 14 8 2 RSDR, Recovery, 12 109 12 98 5 98 RSDr, 10 19 4 RSDR, Recovery, 19 109 24 100 8 100 8
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